HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1977273Generated: November 1, 2026
Potassium Carbonate → HCID 21997462, compound
https://huagongshe.com/reaction/1977273
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Benzene, (3-bromopropoxy)- | HCID 68522 | — |
| Reactant | Methyl 4'-hydroxy(1,1'-biphenyl)-4-carboxylate | HCID 1490289 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21997462 | HCID 21997462 | 81.9% |
Reaction Steps
A solution of methyl 4-(4′-hydroxyphenyl)benzoate (2 g) in N,N-dimethylformamide (20 ml) was treated with potassium carbonate (1.21 g) and 3-phenoxypropylbromide (2.07 g) was stirred for 15 hours at room temperature and 4 hours at 85° C. After cooling, the reaction was quenched with water and the precipitate was collected, washed thoroughly with water and dried to give methyl 4-[4′-(3-phenoxypropyloxy)phenyl]-benzoate (2.6 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06232290B1 |
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| Source dataset | uspto-grants-2001_05 |
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| ORD ID | ord-568be43de9554025850adef369ba1898 |
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| Source note | uspto-grants-2001_05 |
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