HRID1977318
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
An ammonia solution is added to a solution of maltol dissolved in hot distilled water. The pH of this solution is adjusted to 9.8 by the addition of HCl solution. The mixture is kept under reflux overnight and then decolorized with activated charcoal. The solvent is removed under reduced pressure. The white product is obtained upon recrystallization from hot water.
WORKUP
后处理
- dissolutiondissolved
- distillationin hot distilled water
- additionThe pH of this solution is adjusted to 9.8 by the addition of HCl solution
- temperatureunder reflux overnight
- customThe solvent is removed under reduced pressure
- customThe white product is obtained upon recrystallization from hot water