Tert-Butylamine → t-butyl ammonium (R)-3,4epoxybutyrate

Beteiligte Stoffe

Reaktionsschritte

t-butyl amine (571mg, 7.81mmol) was added to the reacting solution of D2O containing (S)-4-hydroxy-3-methanesulfonyl hydroxybutyric acid, so prepared from Example 3 and stirred at room temperature for 4 hours. The presence of the target t-butyl anmmonium (R)-3,4-epoxybutyrate in a layer of the reacting solution was confirmed by nuclear magnetic resonance.

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