HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-1,3-cyclohexanedione → 3-[3-(2-Indanyloxy)-4-methoxyanilino]-2-methyl-2-cyclohexen-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-1,3-cyclohexanedione | HCID 70945 | — |
| Reactant | 3-(2-Indanyloxy)-4-methoxyaniline | HCID 22747743 | — |
| Product | 3-[3-(2-Indanyloxy)-4-methoxyanilino]-2-methyl-2-cyclohexen-1-one | HCID 21994388 | 94.2% |
Reaction Steps
According to the same procedure as in Example 1(3), using 3-(2-indanyloxy)-4-methoxyaniline produced in Example 9(2) instead of 3-cyclopentyloxy-4-methoxyaniline, and using 2-methyl-1,3-cyclohexanedione instead of the 1,3-cyclopentanedione, the title compound (yield 94.2%) was obtained as a light brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235736B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-0046bf8d396d49a781ebb91c02f0e26b |
| Source note | uspto-grants-2001_05 |