HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 135815248, compound → HCID 135815260, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 135815248 | HCID 135815248 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 135815260 | HCID 135815260 | — |
Reaction Steps
Pyridinium chlorochromate (400 mg, 0.00186 mol) was added to a solution of 5-[α-hydroxybenzyl]-1-methyl-3-propyl-6,7-dihydro-1H-pyrazolo[4,3-d]pyrimidin-7-one (200 mg, 0.00068 mol) in dichloromethane (50 ml) and the reaction stirred at room temperature for 3 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235742B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-539c83d80d064650aa46ead962503dc4 |
| Source note | uspto-grants-2001_05 |