HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetanilide → HCID 14319804, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetanilide | HCID 904 | — |
| Reactant | 3-Bromopyridine | HCID 12286 | — |
| Product | HCID 14319804 | HCID 14319804 | 101% |
Reaction Steps
Acetanilide (6.0 g) and 3-bromopyridine (14.1 g) were used to make a reaction in the same manner as in 1) of Production Example 2. The subsequent purification by silica gel column chromatography (developing solvent, ethyl acetate:hexane:=1:1 to 2:1) produced N-(3-pyridyl)-acetanilide (9.52 g, quantitative) as a pale red solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235730B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-7d53c09f742f41d098b10edad91e4ab4 |
| Source note | uspto-grants-2001_05 |