HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodobenzene → 2-ethyl-N-phenylacetanilide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodobenzene | HCID 11575 | — |
| Reactant | N-Phenylbutanamide | HCID 14323 | — |
| Product | 2-ethyl-N-phenylacetanilide | HCID 12666457 | 56% |
Reaction Steps
Using 2-ethylacetanilide (4.9 g) and iodobenzene (12.4 ml), a reaction as made in the same manner as in 1) of Production Example 2. The subsequent purification by silica gel column chromatography (developing solvent, ethyl acetate:hexane=1:3) produced 2-ethyl-N-phenylacetanilide (4.0 g; yield, 56%) as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235730B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-57518f02591e4f799717cc480ff7fd23 |
| Source note | uspto-grants-2001_05 |