HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylacetanilide → HCID 21993578, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylacetanilide | HCID 12107 | — |
| Reactant | 2-Bromo-3-methylpyridine | HCID 220832 | — |
| Product | HCID 21993578 | HCID 21993578 | 99.8% |
Reaction Steps
Using 2-methylacetanilide (4.48 g) and 2-bromo-3-methylpyridine (10.3 g), a reaction was made in the same manner as in 1) of Production Example 14. The subsequent purification by silica gel column chromatography (developing solvent, ethyl acetate: hexane=1:3) produced 2-methyl-N-(3-methyl-2-pyridyl)acetanilide (7.2 g, crude product) as a pale brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235730B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-a3e1fae85b6e4c60b15c7de76427e827 |
| Source note | uspto-grants-2001_05 |