HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 21995277, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 21995297 | HCID 21995297 | — |
| Reactant | HCID 21995324 | HCID 21995324 | — |
| Product | HCID 21995277 | HCID 21995277 | — |
Reaction Steps
In a manner analogous to the preparation of the compound of Example 62 (267 mg, 0.5 mmol) from the compound of Example 106 and LiAlH4 (40 mg, 1.1 mmol) to give the title compound (108 mg) as a light pink solid m.p. 172°. MS m/z 397 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235746B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-8065b9322de04447ba2269e3b2dd1871 |
| Source note | uspto-grants-2001_05 |