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HRID1977957

反应详情

EQUATION

反应方程式

HRID 1977957 的结构方程式

REACTANTS

反应物

2
结构：COc1cc(O)cc(O)c1
HCID71648

Flamenol

C7H8O3

结构：CS(=O)(=O)c1ccccc1S(=O)(=O)Cl
HCID2735178

2-(methylsulfonyl)benzenesulfonyl chloride

C7H7ClO4S2

PRODUCTS

生成物

1
结构：COc1cc(O)cc(OS(=O)(=O)c2ccccc2S(C)(=O)=O)c1
HCID17871222

未命名化合物

收率 80%

PROCEDURE

实验过程

The title compound was prepared in 80% yield from 2-methylsulfonylbenzenesulfonyl chloride and 5-methoxyresorcinol in a manner analogous to step a of Example 1. 1H-NMR (300 MHz, CDCl3) δ8.42 (d, J=7.8 Hz, 1H), 8.13 (d, J=7.8 Hz, 1H), 7.88 (t, J=7.8 Hz, 1H), 7.75 (t, J=7.7 Hz, 1H), 6.36 (s, 1H), 6.31 (s, 1H), 6.28 (s, 1H), 3.68 (s, 3H), 3.45 (s, 3H).