HCID 15712513, compound → HCID 86756744, compound

HRID 1978078Notes

Reaction equation

HRID 1978078 reaction equation
O1CCCCC1[O:7][NH:8][C:9]([C@H:11]([C@@H:21]([CH2:30][CH:31]([CH3:33])[CH3:32])[C:22]([NH:24][NH:25][S:26]([CH3:29])(=[O:28])=[O:27])=[O:23])[CH2:12]/[CH:13]=[CH:14]/[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[O:10].CS(O[CH2:39][CH:40]1[CH2:44][CH2:43][CH2:42][CH2:41]1)(=O)=O>>[CH:40]1([CH2:39][N:25]([S:26]([CH3:29])(=[O:27])=[O:28])[NH:24][C:22](=[O:23])[C@@H:21]([C@@H:11]([C:9](=[O:10])[NH:8][OH:7])[CH2:12]/[CH:13]=[CH:14]/[C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)[CH2:30][CH:31]([CH3:32])[CH3:33])[CH2:44][CH2:43][CH2:42][CH2:41]1

Participants

3

Reactant 2

HCID 15712513HCID 15712513, compoundHCID 86756723HCID 86756723, compound

Product 1

HCID 86756744HCID 86756744, compound

Procedure

The starting material was prepared in an analogous manner to that described in Example 15, part (iii), starting from (E)-2(R)-[1(S)-[(tetrahydro-2(RS)-pyranyloxy)carbamoyl]-4-phenyl-3-butenyl]-2′-(methanesulphonyl)-4-methylvalerohydrazide and cyclopentylmethyl methanesulphonate.

Workup

  1. customThe starting material was prepared in an analogous manner to that

Sources & evidence

ORD record
ord-6a69e7d6c73441c891b2cf5da6d55854
Source dataset
uspto-grants-2001_05
Patent number
US06235787B1

Reaction notes

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