Acrylic Acid → HCID 66766855, compound

Participants

Reaction Steps

To 200 ml of toluene were added 0.1 mole of 1-hydroxyadamantane, 0.2 mole of acrylic acid, 0.06 mole of p-toluene sulfinic acid and 0.2 mole of p-methoxyphenol, and the resultant mixture was stirred at the reflux temperature to esterify reacted while collecting the provided water to the point where the amount of produced water reached the theoretical amount. The reaction product was neutralized by 10 parts by weight of sodium hydroxide solution, and the precipitate produced was separated by filtration, and the toluene was distilled off under reduced pressure. The resultant crude product was recrystalized from n-hexane to obtain an adamantane monoacrylate.

Provenance & Evidence