HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dihydroxyadamantane-1-carboxylic acid → 1-Carboxy-3-hydroxy-5-acryloyloxyadamantane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dihydroxyadamantane-1-carboxylic acid | HCID 12010647 | — |
| Reactant | 1-Hydroxy-3-(acryloyloxymethyl)adamantane | HCID 21996783 | — |
| Product | 1-Carboxy-3-hydroxy-5-acryloyloxyadamantane | HCID 22650054 | 84% |
Reaction Steps
The reaction was conducted in the same manner as the step of Example 36 (2) except that 1-carboxy-3,5-dihydroxyadamantane was used instead of the 1,3-dicarboxy-5-adamantanol, and, as a result, a 1-carboxy-3-hydroxy-5-acryloyloxyadamantane (yield: 84%, white solid) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235851B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-817ef89dd7d44f47bb21758f0968af33 |
| Source note | uspto-grants-2001_05 |