HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3,5,7-Tetrahydroxyadamantane → 1,3,5-Trihydroxy-7-acryloyloxyadamantane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3,5,7-Tetrahydroxyadamantane | HCID 820093 | — |
| Reactant | 1-Hydroxy-3-(acryloyloxymethyl)adamantane | HCID 21996783 | — |
| Product | 1,3,5-Trihydroxy-7-acryloyloxyadamantane | HCID 21996790 | 83% |
Reaction Steps
The reaction was conducted in the same manner as the step of Example 36 (2) except that 1,3,5,7-tetrahydroxyadamantane was used instead of the 1,3-dicarboxy-5-adamantanol, and, as a result, a 1,3,5-trihydroxy-7-acryloyloxyadamantane (yield: 83%, white solid) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235851B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-40d3d6ff280a48f29989019d35165277 |
| Source note | uspto-grants-2001_05 |