HCID 12572978, compound → HCID 15022710, compound

HRID 1978147Notes

Reaction equation

HRID 1978147 reaction equation
[Cl:1][C:2]1[N:7]=[C:6]([O:8][CH:9]([Cl:11])[Cl:10])[CH:5]=[C:4]([C:12]([Cl:15])([Cl:14])[Cl:13])[N:3]=1.[Cl:16]C1N=C(Cl)C=C(C(Cl)(Cl)Cl)N=1>>[Cl:1][C:2]1[N:7]=[C:6]([O:8][C:9]([Cl:16])([Cl:10])[Cl:11])[CH:5]=[C:4]([C:12]([Cl:15])([Cl:13])[Cl:14])[N:3]=1

Participants

3

Reactant 2

HCID 12572978HCID 12572978, compoundHCID 21996896HCID 21996896, compound

Product 1

HCID 15022710HCID 15022710, compoundYield 83%

Procedure

The gas chromatogram of the filtrate (113.8 g) showed that it was composed of 83% title compound, 4% 2-chloro-4-dichloromethoxy-6-trichloromethylpyrimidine and 9% 2,4-dichloro-6-trichloromethylpyrimidine. The total yield of the title compound was 87.6% of theory.

Sources & evidence

ORD record
ord-c27da2d6d63540478f371e4385c0cf48
Source dataset
uspto-grants-2001_05
Patent number
US06235904B1

Reaction notes

Loading…