HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stearyl Alcohol → HCID 15405269, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stearyl Alcohol | HCID 8221 | — |
| Reactant | 2-Methoxypropene | HCID 8300 | — |
| Catalyst | Triethylamine | HCID 8471 | — |
| Catalyst | Phosphorus oxychloride | HCID 24813 | — |
| Product | HCID 15405269 | HCID 15405269 | — |
Reaction Steps
2-methoxy-2-(octadecyloxy)propane was prepared by reacting stearic alcohol (0.025 mole) with 2-methoxypropene (4 equivalents) for 2 hours at 20° C. in the presence of one drop of phosphoryl chloride (POCl3) then adding 5 drops of triethylamine and distilling the excess enol ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235956B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-e644f463808544deaf8e93123f444758 |
| Source note | uspto-grants-2001_05 |