Hydrochloride methanol → HCID 21993952, compound

Participants

Reaction Steps

To a solution of 1.84 g (4.25 mM) of N-[3-(4-benzylpiperidin-1-yl)propan-1-yl]-5-thia-1,8b-diazaacenaphthylene-4-carboxamide in ethanol (10 ml) was added 6 ml (24 mM) of 4N-HCl/methanol at room temperature and the mixture was stirred at room temperature for several minutes. After the solvent was distilled off under reduced pressure, ethanol and diethyl ether were added to the crystalline residue. The crystal crop was then harvested by filtration and rinsed with ethanol and diethyl ether to provide the title compound as orange-colored crystals.

Provenance & Evidence