Hydrochloride methanol → HCID 21993848, compound

Participants

Reaction Steps

To a solution of 0.8113 g (1.76 mM) of N-[3-(1-(3-phenylpropan-1-yl)piperidin-4-yl)propan-1-yl]-5-thia-1,8b-diazaacenaphthylene-4-carboxamide in ethanol (10 ml) was added 6 ml (24 mM) of 4N-HCl/methanol at room temperature and the mixture was stirred at room temperature for several minutes. The solvent was then distilled off under reduced pressure, and after addition of diethyl ether to the crystalline residue, the crystal crop was harvested by filtration and rinsed with ethanol and diethyl ether to provide the title compound.

Provenance & Evidence