HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminophenylacetic acid → 4-((((2-Methylphenyl)amino)carbonyl)amino)benzeneacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminophenylacetic acid | HCID 14533 | — |
| Reactant | 2-Tolyl isocyanate | HCID 69194 | — |
| Product | 4-((((2-Methylphenyl)amino)carbonyl)amino)benzeneacetic acid | HCID 6605254 | — |
Reaction Steps
4-o-Tolylureidophenylacetic acid was prepared using procedure C with 4-amino-phenylacetic acid and o-tolyl isocyanate: 1H NMR (CD3SOCD3, 300 MHz, ppm) 8.97 (s, 1H), 7.88 (s, 1H), 7.83 (d, 1H), 7.38 (d, 2H), 7.17-7.09 (m, 4H), 6.92 (t, 1H), 3.48 (s, 2H), 2.23 (s, 3H); m/z 285.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06239108B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-4f860c4b046d4673b3aedb97bab28f63 |
| Source note | uspto-grants-2001_05 |