HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21993065, compound → HCID 15789650, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21993065 | HCID 21993065 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 15789650 | HCID 15789650 | 76.2% |
Reaction Steps
A solution of 2.09 g (6.1 mmol) of N-tert-butyl-5-acetamidomethyl-2-methoxycarbonylbenzenesulfonamide in 25 ml of trifluoroacetic acid is stirred at room temperature for 14 h and then evaporated to dryness. Crystallization of the residue from ethyl acetate yields 1.33 g (76%) of 5-acetamidomethyl-2-methoxycarbonylbenzenesulfonamide of mp. 173-175° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06239306B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-d11a39864d1f42c9bce31181a28185b5 |
| Source note | uspto-grants-2001_05 |