HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86756975, compound → HCID 20658011, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86756975 | HCID 86756975 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20658011 | HCID 20658011 | 97.1% |
Reaction Steps
A solution of 0.880 g of benzyl-2(R)-[3-azido-1(S)-(tert-butoxycarbonyl)propyl]-4-methylvalerate in 10 ml of ethanol was hydrogenated in the presence of 0.090 g of 5% palladium-on-carbon for 12 hours. The catalyst was removed by filtration and the solvent was evaporated to give 0.600 g of 2(R)-[3-amino-1(S)-(tert-butoxycarbonyl)propyl]-4-methylvaleric acid in the form of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06239151B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-15ef7a946dca4516bb70d822cf29277d |
| Source note | uspto-grants-2001_05 |