Crotyl chloride → HCID 53866210, compound

HRID 1979504Notes

Reaction equation

[CH2:1]([C:8]([CH2:10][CH3:11])=[O:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:12](Cl)[CH:13]=[CH:14][CH3:15]>>[C:2]1([CH:1]([C:8](=[O:9])[CH2:10][CH3:11])[CH2:12][CH:13]=[CH:14][CH3:15])[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 11589Crotyl chloride

HCID 138791-Phenyl-2-butanone

Product 1

HCID 53866210HCID 53866210, compound

Procedure

Ethyl benzyl ketone is reacted with crotyl chloride according to the foregoing details and there is obtained 5-phenyl-oct-2-en-6-one of boiling point 95° C./3 mmHg; nD20 =1.5102.

Sources & evidence

ORD record: ord-e02f288308a846ce9f156313da4d5510
Source dataset: uspto-grants-1984_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04481133

Reaction notes

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