4-Chloro-1-(chloromethyl)-2-methylbenzene → 1-Decyl-3-[2-methyl-4-chlorobenzyl]-4-methyl-5-chloroimidazolium chloride
Reaction equation
[CH2:1]([N:11]1[C:15]([Cl:16])=[C:14]([CH3:17])[N:13]=[CH:12]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[CH3:18][C:19]1[CH:26]=[C:25]([Cl:27])[CH:24]=[CH:23][C:20]=1[CH2:21]Cl>>[Cl-:16].[CH2:1]([N+:11]1[C:15]([Cl:16])=[C:14]([CH3:17])[N:13]([CH2:21][C:20]2[CH:23]=[CH:24][C:25]([Cl:27])=[CH:26][C:19]=2[CH3:18])[CH:12]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]Participants
3
Conditions
- Temperature
- 125 °C
Procedure
25.6 g (0.1 mole) of 1-decyl-4-methyl-5-chloroimidazole were heated to 100° C., 17.7 g (0.1 mole ) of 4-chloro-o-xylyl chloride were added dropwise, and the mixture was stirred for a further 30 minutes at 125° C.
Sources & evidence
- ORD record
- ord-1a839c50e5d74d698217605ba387b76f
- Source dataset
- uspto-grants-1984_11
- Patent number
- US04481211
Reaction notes
Loading…