Benzyl Chloride → 1-Decyl-3-benzyl-4-methyl-5-chloroimidazolium chloride

HRID 1979530Notes

Reaction equation

[CH2:1]([N:11]1[C:15]([Cl:16])=[C:14]([CH3:17])[N:13]=[CH:12]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[CH2:18](Cl)[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[Cl-:16].[CH2:1]([N+:11]1[C:15]([Cl:16])=[C:14]([CH3:17])[N:13]([CH2:18][C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[CH:12]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

Reactant 2

HCID 7503Benzyl Chloride

HCID 131950791-Decyl-4-methyl-5-chloroimidazole

Product 1

HCID 867397481-Decyl-3-benzyl-4-methyl-5-chloroimidazolium chloride

Conditions

Temperature: 125 °C

Procedure

25.5 g (0.1 mole) of 1-decyl-4-methyl-5-chloroimidazole were heated to 100° C., 12.6 g (0.1 mole) of benzyl chloride were added dropwise in the course of 10 minutes, and the mixture was then stirred for a further 30 minutes at 125° C.

Sources & evidence

ORD record: ord-7006f335b21e495ba14f18e80fa9d08e
Source dataset: uspto-grants-1984_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04481211

Reaction notes

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