Styrene → Butyl prop-2-enoate;styrene

HRID 1979596Notes

Reaction equation

HRID 1979596 reaction equation
[CH2:1]([O:5][C:6](=[O:9])[CH:7]=[CH2:8])[CH2:2][CH2:3][CH3:4].[CH2:10]=[CH:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.S(OOS([O-])(=O)=O)([O-])(=O)=O.[Na+].[Na+]>O>[CH2:1]([O:5][C:6](=[O:9])[CH:7]=[CH2:8])[CH2:2][CH2:3][CH3:4].[CH2:10]=[CH:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

5

Reactant 3

HCID 7501StyreneHCID 8846Butyl AcrylateHCID 62655Sodium Persulfate

Product 1

HCID 168422Butyl prop-2-enoate;styrene

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A butylacrylate/styrene latex is prepared by emulsifying by stirring in the presence of the wetting agent a mixture of 18.6 g of butylacrylate and 21.2 g of styrene in 50 g of water and initiating the polymerisation, at 70° C. under nitrogen, with 0.13 g of sodium persulphate. The latex so prepared contains 47% by weight of solids.

Workup

  1. customthe polymerisation
  2. customat 70° C.
  3. customThe latex so prepared

Sources & evidence

ORD record
ord-88e939a44fcc4874856ffc8f31e4d643
Source dataset
uspto-grants-1984_11
Patent number
US04481252

Reaction notes

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