HuagongsheHuagongshe Chemistry Print Report · For research reference only
Furfuryl Alcohol → HCID 20274631, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Furfuryl Alcohol | HCID 7361 | — |
| Reactant | Dimethyl malonate | HCID 7943 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20274631 | HCID 20274631 | — |
Reaction Steps
196 parts by wt. of furfuryl alcohol and 132 parts by wt. dimethyl malonate (stoichiometric proportions) are mixed and 0.5-0.75% wt. sodium metal added. The mixture is heated to a temperature in the range from 214°-240° F. under a nitrogen atmoshpere. Methanol is evolved and removed as the reaction progressed. After a period of 4 hours, a waxy solid is obtained. The liquid product obtained after washing with water is difurfuryl malonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04481310 |
| Source dataset | uspto-grants-1984_11 |
| ORD ID | ord-50087a871bf547c39e5823bdc6586a18 |
| Source note | uspto-grants-1984_11 |