HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → 2,5-Cyclohexadiene-1,4-dione, 2,3,5-trimethyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 2,3,5-Trimethylphenol | HCID 12769 | — |
| Product | 2,5-Cyclohexadiene-1,4-dione, 2,3,5-trimethyl- | HCID 70291 | 51% |
Reaction Steps
500 mg of 2,3,5-trimethylphenol and 10 mg of RuCl3.3H2O was reacted in 5 ml of acetic acid in the same manner as in Example 1, followed by the same treatment as in Example 1, whereby 100 mg of unreacted starting material and 230 mg (51% yield) of trimethylbenzoquinone was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04482493 |
| Source dataset | uspto-grants-1984_11 |
| ORD ID | ord-e29861569e8148afb4c67106a87a4ede |
| Source note | uspto-grants-1984_11 |