HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl 1-aminocyclopentane-1-carboxylate → HCID 13376657, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl 1-aminocyclopentane-1-carboxylate | HCID 231228 | — |
| Reactant | 4-Methoxy-2-methyl-4-oxobutanoic acid | HCID 4563901 | — |
| Product | HCID 13376657 | HCID 13376657 | — |
Reaction Steps
1-[(3-Methoxycarbonyl-2-methylpropanoyl)amino]-1-cyclopentanecarboxylic acid, benzyl ester was prepared as described in Example 3 from 10.96 g (0.050 mol) of 1-amino-1-cyclopentanecarboxylic acid, benzyl ester and 7.31 g (0.050 mol) of 3-methoxycarbonyl-2-methylpropionic acid. Crude di-ester crystallized to give 13.57 g (78%) of an off-white solid, mp: 88°-93°. This was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04482572 |
| Source dataset | uspto-grants-1984_11 |
| ORD ID | ord-6e38844d57004eafbada95de2f3d7f27 |
| Source note | uspto-grants-1984_11 |