2-Nitrobenzaldehyde → HCID 53717727, compound

HRID 1979800Notes

Reaction equation

[N+:1]([C:4]1[CH:11]=[CH:10][CH:9]=[CH:8][C:5]=1[CH:6]=O)([O-:3])=[O:2].[NH2:12][CH2:13][P:14]([C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)(=[O:19])[O:15][CH:16]([CH3:18])[CH3:17]>>[N+:1]([C:4]1[CH:11]=[CH:10][CH:9]=[CH:8][C:5]=1[CH:6]=[N:12][CH2:13][P:14]([C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)(=[O:19])[O:15][CH:16]([CH3:18])[CH3:17])([O-:3])=[O:2]

Participants

Reactant 2

HCID 111012-Nitrobenzaldehyde

HCID 13740520HCID 13740520, compound

Product 1

HCID 53717727HCID 53717727, compoundYield 100%

Procedure

Starting from 0.1 mol o-nitrobenzaldehyde and 0.1 mol isopropyl aminomethyl-phenylphosphinate, 0.1 mol (100%) of the desired imine is obtained (by following the procedure described in Example 1) in the form of a yellow oil.

Sources & evidence

ORD record: ord-81a20a2c07ce4b52b7b9ec30240ad075
Source dataset: uspto-grants-1984_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04482718

Reaction notes

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