HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Cresol → 2,6-Dimethylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Cresol | HCID 335 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Phenol | HCID 996 | — |
| Solvent | Nitrogen | HCID 947 | — |
| Product | 2,6-Dimethylphenol | HCID 11335 | 34% |
Reaction Steps
29.5 g of the catalyst is charged with a 5/1 moles methanol/mole phenol mixture with LHSV of 0.68 h-1. The gaseous mixture, diluted with N2 as the carrier gas after its vaporization at 140° C., is converted to an extent of 83% at 372° C. The yield is 34% of 2,6-dimethylphenol and 47% of o-cresol. After an operating period of 40 hours, the catalyst activity and selectivity decrease sharply.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04482758 |
| Source dataset | uspto-grants-1984_11 |
| ORD ID | ord-7b13e368a3d2422fbd3be1ca39cc2912 |
| Source note | uspto-grants-1984_11 |