HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20405767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-Butanesulfonic acid, 4-hydroxy- | HCID 112575 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 20405767 | HCID 20405767 | — |
Reaction Steps
Sulfoalkylating agent, obtainable by heating 4-hydroxy butane-2-sulfonic acid or 3-methyl-1,3-propane sultone to a temperature in the region of from 80° to 180° C. in the presence of water in an amount of from 1 to 4 moles per mol of 4-hydroxy-butane-2-sulfonic acid or 3-methyl-1,3-propane sultone, and characterized by the following 13C-NMR-shifts (ppm, relative to TMS=0, in the presence of dioxane): 15.4; 31.7; 34.4; 53.6; 60.0 and 68.5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04483799 |
| Source dataset | uspto-grants-1984_11 |
| ORD ID | ord-fcc94fe4523f41a4b8e6b856077b2732 |
| Source note | uspto-grants-1984_11 |