HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glyoxylic Acid → HCID 12810649, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glyoxylic Acid | HCID 760 | — |
| Reactant | 2',5'-Dimethoxyacetophenone | HCID 70991 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 12810649 | HCID 12810649 | — |
Reaction Steps
22.2 g of glyoxylic acid, 50 wt.% in water, are heated under reduced pressure until about 80% of the water present has been eliminated; then, after cooling, 54 g of 2,5-dimethoxyacetophenone are added, i.e., an excess of 100% over theoretical.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04483868 |
| Source dataset | uspto-grants-1984_11 |
| ORD ID | ord-f2883e041b87416881f91512851bf80b |
| Source note | uspto-grants-1984_11 |