Acetic Acid → HCID 3069393, compound

HRID 1979956Notes

Reaction equation

HRID 1979956 reaction equation
[C:1]([OH:5])(=[O:4])[CH:2]=O.[CH2:6]1[O:14][C:13]2[CH:12]=[CH:11][C:10]([C:15](=[O:17])[CH3:16])=[CH:9][C:8]=2[O:7]1.C(O)(=O)C>O>[CH2:6]1[O:14][C:13]2[CH:12]=[CH:11][C:10]([C:15](=[O:17])[CH:16]=[CH:2][C:1]([OH:5])=[O:4])=[CH:9][C:8]=2[O:7]1

Participants

5

Reactant 3

HCID 176Acetic AcidHCID 760Glyoxylic AcidHCID 76622Acetopiperone

Product 1

HCID 3069393HCID 3069393, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

44 g of glyoxylic acid, 50 wt.% in water, are heated under reduced pressure to eliminate the major part (80%) of the water present; there are then introduced into the reaction medium 49.2 g of 3',4'-methylenedioxy-acetophenone, and 100 cm3 of acetic acid.

Sources & evidence

ORD record
ord-95426a4d53354c5a9928384238de0525
Source dataset
uspto-grants-1984_11
Patent number
US04483868

Reaction notes

Loading…