HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diphenyl Ether → 1-Propanone, 1,1'-(oxydi-4,1-phenylene)bis-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diphenyl Ether | HCID 7583 | — |
| Reactant | Propionyl chloride | HCID 62324 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Carbon Disulfide | HCID 6348 | — |
| Product | 1-Propanone, 1,1'-(oxydi-4,1-phenylene)bis- | HCID 10684295 | — |
Reaction Steps
Diphenyl ether (67 grams) was mixed with about 79 grams of propionyl chloride and 109 grams of aluminum chloride in about 150 ml of carbon disulfide. The product, 4-propionylphenyl ether, was isolated by hydrolysis of the mixture and conventional recrystallization techniques.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04483984 |
| Source dataset | uspto-grants-1984_11 |
| ORD ID | ord-306e3264f3054b1194b6e8b12b767234 |
| Source note | uspto-grants-1984_11 |