Octanoyl chloride → HCID 13363154, compound

HRID 1979990Notes

Reaction equation

[OH:1][CH2:2][CH2:3][C:4]1[C:5]2[N:6]([N:17]=[CH:18][N:19]=2)[C:7]([NH2:16])=[N:8][C:9]=1[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1.[C:20](Cl)(=[O:28])[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27]>>[C:20]([O:1][CH2:2][CH2:3][C:4]1[C:5]2[N:6]([N:17]=[CH:18][N:19]=2)[C:7]([NH2:16])=[N:8][C:9]=1[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)(=[O:28])[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27]

Participants

Reactant 2

HCID 8124Octanoyl chloride

HCID 175635Sc-36741

Product 1

HCID 13363154HCID 13363154, compound

Procedure

The title compound, m.p. 89°-91°, was prepared by the method of Example 2 using 5.1 g (0.02 mole) of the product compound of Example 1 and 3.25 g (0.02 mole) of octanoyl chloride, except that the solution was not divided before purification.

Sources & evidence

ORD record: ord-9588f097f38d432fad1b767f9f18bbf3
Source dataset: uspto-grants-1984_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04483987

Reaction notes

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