HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-methoxy-1,4-dimethyl-9H-carbazole → 6-Hydroxy-1,4-dimethylcarbazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-methoxy-1,4-dimethyl-9H-carbazole | HCID 87416 | — |
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Product | 6-Hydroxy-1,4-dimethylcarbazole | HCID 194331 | — |
Reaction Steps
A solution of 30 g of 6-methoxy-1,4-dimethyl-carbazole in 300 g of absolutely anhydrous (water-free) pyridine hydrochloride was heated with gentle reflux on 180°-190° C. for 5 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04483989 |
| Source dataset | uspto-grants-1984_11 |
| ORD ID | ord-c15bbfb3834c4dcda98199fcd1ed5921 |
| Source note | uspto-grants-1984_11 |