HRID1980105
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
To a solution of 1.35 g of methallyl chloride in 25 ml of methylene chloride was added 2.15 g of N-methyl-N-chlorosulfenyl carbamoyl fluoride. The solution was heated to reflux for 45 min. and concentrated to 1.68 g of pale yellow oil.
WORKUP
后处理
- temperatureThe solution was heated
- temperatureto reflux for 45 min.
- concentrationconcentrated to 1.68 g of pale yellow oil