HRID1980105

反应详情

EQUATION

反应方程式

HRID 1980105 的结构方程式

PROCEDURE

实验过程

To a solution of 1.35 g of methallyl chloride in 25 ml of methylene chloride was added 2.15 g of N-methyl-N-chlorosulfenyl carbamoyl fluoride. The solution was heated to reflux for 45 min. and concentrated to 1.68 g of pale yellow oil.

WORKUP

后处理

  1. temperatureThe solution was heated
  2. temperatureto reflux for 45 min.
  3. concentrationconcentrated to 1.68 g of pale yellow oil