HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-(14-Methylpentadecyl)aminobenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Ethyl 4-(14-methylpentadecyl)aminobenzoate | HCID 20437387 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4-(14-Methylpentadecyl)aminobenzoic acid | HCID 20437364 | — |
Reaction Steps
A 4 g. sample of ethyl 4-(14-methylpentadecyl)aminobenzoate is hydrolized with 2.0 g. of 85% potassium hydroxide in 60 ml. 95% ethanol by refluxing the solution for 5 hours. The solution is cooled, diluted with 100 ml. water, and acidified to pH 4.5 with 37% hydrochloric acid. The precipitate is collected and dried in vacuo to yield the title compound as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04485105 |
| Source dataset | uspto-grants-1984_11 |
| ORD ID | ord-23f0cc27d6b1403ba1d9f7ed323dbca6 |
| Source note | uspto-grants-1984_11 |