HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-(13,13-Dimethyltetradecyl)aminobenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Ethyl 4-(13,13-dimethyltetradecyl)aminobenzoate | HCID 20437372 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4-(13,13-Dimethyltetradecyl)aminobenzoic acid | HCID 20437343 | — |
Reaction Steps
A solution of 5 g. of ethyl 4-(13,13-dimethyltetradecyl)aminobenzoate in 75 ml. 95% ethanol is saponified with 2.5 g. of 85% potassium hydroxide by refluxing for 5 hours. The warm solution is diluted with 150 ml. water and adjusted to pH 5 with 37% hydrochloric acid. The precipitate is filtered, washed with water, dried in vacuo and crystallized from acetic acid to yield the title compound as a cream-colored, amorphous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04485105 |
| Source dataset | uspto-grants-1984_11 |
| ORD ID | ord-6c68aef8b29c40c5bc1a92723d9a1c06 |
| Source note | uspto-grants-1984_11 |