Neopentyl glycol → HCID 13634432, compound

HRID 1980430Notes

Reaction equation

HRID 1980430 reaction equation
Cl[C:2]([O:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[O:11][CH3:12])=[O:3].[CH3:13][C:14]([CH3:19])([CH2:17][OH:18])[CH2:15][OH:16].ClC([O-])=O>>[CH3:12][O:11][C:6]1[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=1[O:4][C:2]([O:16][CH2:15][C:14]([CH3:19])([CH3:13])[CH2:17][OH:18])=[O:3]

Participants

4

Reactant 3

HCID 31344Neopentyl glycolHCID 33621432-Methoxyphenyl chloroformateHCID 21226386Carbonochloridate

Product 1

HCID 13634432HCID 13634432, compound

Procedure

The reaction of 2-methoxyphenol chloroformate with 2,2-dimethyl-1,3-propanediol is conducted on a 0.01 mole scale employing the same conditions as described in Example III, except that the addition of the chloroformate solution is accomplished at room temperature. A 1.4 g yield of the pure product is obtained as an oil.

Workup

  1. customis accomplished at room temperature
  2. customA 1.4 g yield of the pure product is obtained as an oil

Sources & evidence

ORD record
ord-26b5c5e332a64ab7abd25be7d527366a
Source dataset
uspto-grants-1985_04
Patent number
US04509537

Reaction notes

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