2,4-Pentanediol → HCID 13634433, compound
Reaction equation
Cl[C:2]([O:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[O:11][CH3:12])=[O:3].[CH3:13][CH:14]([OH:19])[CH2:15][CH:16]([OH:18])[CH3:17]>>[CH3:12][O:11][C:6]1[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=1[O:4][C:2]([O:18][CH:16]([CH2:15][CH:14]([OH:19])[CH3:13])[CH3:17])=[O:3]Participants
3
Procedure
The reaction of 2-methoxyphenol chloroformate with 2,4-pentanediol is conducted on a 0.01 mole scale employing the same conditions as described in Example III. A 1.5 g yield of the pure product is obtained as an oil.
Workup
- customA 1.5 g yield of the pure product is obtained as an oil
Sources & evidence
- ORD record
- ord-50c2e876e092480b930e075411bd4f50
- Source dataset
- uspto-grants-1985_04
- Patent number
- US04509537
Reaction notes
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