Neopentyl glycol → HCID 20401562, compound
Reaction equation
Cl[C:2]([O:4][C:5]1[CH:10]=[C:9]([CH3:11])[CH:8]=[CH:7][C:6]=1[CH:12]([CH3:14])[CH3:13])=[O:3].[CH3:15][C:16]([CH3:21])([CH2:19][OH:20])[CH2:17][OH:18]>>[CH:12]([C:6]1[CH:7]=[CH:8][C:9]([CH3:11])=[CH:10][C:5]=1[O:4][C:2]([O:18][CH2:17][C:16]([CH3:21])([CH3:15])[CH2:19][OH:20])=[O:3])([CH3:14])[CH3:13]Participants
3
Procedure
The reaction of 2-isopropyl-5-methylphenyl chloroformate with 2,2-dimethyl-1,3-propanediol is conducted on a 0.01 mole scale employing the same conditions as described in Example I. A 1.3 g yield of the pure product is obtained as an oil.
Workup
- customA 1.3 g yield of the pure product is obtained as an oil
Sources & evidence
- ORD record
- ord-f3b5171fb66f432f8e42d145b072d4e7
- Source dataset
- uspto-grants-1985_04
- Patent number
- US04509537
Reaction notes
Loading…