1,4-Butanediol → HCID 13634428, compound

HRID 1980433Notes

Reaction equation

HRID 1980433 reaction equation
Cl[C:2]([O:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[O:11][CH3:12])=[O:3].[CH2:13]([OH:18])[CH2:14][CH2:15][CH2:16][OH:17]>>[CH3:12][O:11][C:6]1[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=1[O:4][C:2]([O:17][CH2:16][CH2:15][CH2:14][CH2:13][OH:18])=[O:3]

Participants

3

Reactant 2

HCID 80641,4-ButanediolHCID 33621432-Methoxyphenyl chloroformate

Product 1

HCID 13634428HCID 13634428, compound

Procedure

The reaction of 2-methoxyphenyl chloroformate with 1,4-butanediol is conducted on a 0.01 scale employing the same conditions as described in Example IV. A 1.5 g yield of the pure product is obtained as an oil.

Workup

  1. customA 1.5 g yield of the pure product is obtained as an oil

Sources & evidence

ORD record
ord-88617d72c5f6420d980e1748fca2282a
Source dataset
uspto-grants-1985_04
Patent number
US04509537

Reaction notes

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