2,4-Pentanediol → HCID 13634434, compound
Reaction equation
Cl[C:2]([O:4][C:5]1[CH:10]=[CH:9][C:8]([CH:11]=[O:12])=[CH:7][C:6]=1[O:13][CH3:14])=[O:3].[CH3:15][CH:16]([OH:21])[CH2:17][CH:18]([OH:20])[CH3:19]>>[CH3:14][O:13][C:6]1[CH:7]=[C:8]([CH:11]=[O:12])[CH:9]=[CH:10][C:5]=1[O:4][C:2]([O:20][CH:18]([CH2:17][CH:16]([OH:21])[CH3:15])[CH3:19])=[O:3]Participants
3
Procedure
The reaction of 2-methoxy-4-formylphenyl chloroformate with 2,4-pentanediol is conducted on a 0.02 mole scale employing the same conditions as described in Example I. A 2.9 g yield of the pure product is obtained as an oil.
Workup
- customA 2.9 g yield of the pure product is obtained as an oil
Sources & evidence
- ORD record
- ord-e3412b5ae55149bda2da01a602c7bec1
- Source dataset
- uspto-grants-1985_04
- Patent number
- US04509537
Reaction notes
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