2-Methoxyphenyl chloroformate → HCID 13634426, compound

HRID 1980436Notes

Reaction equation

HRID 1980436 reaction equation
Cl[C:2]([O:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[O:11][CH3:12])=[O:3]>C(O)CO>[CH3:12][O:11][C:6]1[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=1[O:4][C:2]([O:4][CH2:5][CH2:6][OH:11])=[O:3]

Participants

3

Reactant 1

HCID 33621432-Methoxyphenyl chloroformate

Product 1

HCID 13634426HCID 13634426, compound

Reagents, catalysts & solvents 1

HCID 174Ethylene GlycolSolvent

Procedure

The reaction of 2-methoxyphenyl chloroformate with ethylene glycol is conducted on a 0.01 mole scale employing the same conditions as described in Example III. A 0.7 g yield of the pure product is obtained as an oil. The product is unstable and decomposes quantitatively after standing at room temperature for several hours.

Workup

  1. customA 0.7 g yield of the pure product is obtained as an oil
  2. waitafter standing at room temperature for several hours

Sources & evidence

ORD record
ord-0fb901ebaad44159bcf5129d2183a6f8
Source dataset
uspto-grants-1985_04
Patent number
US04509537

Reaction notes

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