HuagongsheHuagongshe Chemistry Print Report · For research reference only
Quinone → HCID 20401718, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Quinone | HCID 4650 | — |
| Reactant | 1,3-Butadiene | HCID 7845 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Benzene | HCID 241 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20401718 | HCID 20401718 | — |
Reaction Steps
The reaction was conducted using a solution of p-benzoquinone and each of the above-mentioned butadiene derivatives in benzene under heating and refluxing conditions for four hours. The resulting compounds were dissolved in ethanol, in which was suspended a palladium catalyst adsorbed on alumina. Thereafter, hydrogen gas was blown into the solution for 2 hours while keeping the temperature of the solution at 20° C. to obtain dodecahydro-9,10-anthraquinone derivatives.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04510089 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-ea67bd4cc522423ba059c7b6c58aff80 |
| Source note | uspto-grants-1985_04 |