HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,3-Dimethylaniline → N-(2,3-dimethylphenyl)-2-nitroaniline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,3-Dimethylaniline | HCID 6893 | — |
| Edukt | 1-Fluoro-2-nitrobenzene | HCID 73895 | — |
| Lösungsmittel | Dimethyl Sulfoxide | HCID 679 | — |
| Produkt | N-(2,3-dimethylphenyl)-2-nitroaniline | HCID 13519320 | — |
Reaktionsschritte
In an entirely analogous manner, using 117.00 g (0.830 mol) of 1-fluoro-2-nitrobenzene and 222.00 g (1.826 mol) of 2,3-dimethylaniline in 585 ml of dimethyl sulphoxide as starting materials there is obtained N-(2,3-dimethylphenyl)-2-nitroaniline having a melting point of 118°-120° after recrystallisation from methylene chloride/hexane.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04510141 |
| Quelldatensatz | uspto-grants-1985_04 |
| ORD ID | ord-64b5a115bf924ee2851c55a2443b6c64 |
| Quellennotiz | uspto-grants-1985_04 |