Methanol → HCID 131714190, compound

HRID 1980565Notes

Reaction equation

HRID 1980565 reaction equation
CO.Cl[Si:4](Cl)(Cl)[CH2:5][CH2:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][N:8]=1>O>[SiH3:4][CH2:5][CH2:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][N:8]=1

Participants

4

Reactant 2

HCID 887MethanolHCID 869362-[2-(Trichlorosilyl)ethyl]pyridine

Product 1

HCID 131714190HCID 131714190, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A solution of 2-(2-silylethyl)pyridine oligosilsesquioxane pillar material was prepared from a methanol solution of 2-(2-trichlorosilylethyl)pyridine (24 grams of 2-(2-trichlorosilylethyl)pyridine in 175 ml of methanol) by adding 10.5 ml of water. The mixture was stirred for 1 hour while maintaining the temperature below 30° C.

Workup

  1. temperaturewhile maintaining the temperature below 30° C.

Sources & evidence

ORD record
ord-3632116738ab40bdaa6d721e7104e28e
Source dataset
uspto-grants-1985_04
Patent number
US04510257

Reaction notes

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