1-Chloro-2-phenylethane → HCID 20402309, compound

HRID 1980600Notes

Reaction equation

HRID 1980600 reaction equation
[S:1]([NH:5][S:6]([C:9]1[CH:14]=[CH:13][C:12]([CH:15]=[CH2:16])=[CH:11][CH:10]=1)(=[O:8])=[O:7])([CH3:4])(=[O:3])=[O:2].C1(CC[Cl:25])C=CC=CC=1>>[S:1]([NH:5][S:6]([C:9]1[CH:14]=[CH:13][C:12]([CH2:15][CH2:16][Cl:25])=[CH:11][CH:10]=1)(=[O:7])=[O:8])([CH3:4])(=[O:2])=[O:3]

Participants

3

Reactant 2

HCID 2314961-Chloro-2-phenylethaneHCID 202428244-Ethenyl-N-(methanesulfonyl)benzene-1-sulfonamide

Product 1

HCID 20402309HCID 20402309, compound

Procedure

A procedure similar to that described in Example I was used to prepare the N-mesyl-4-vinylbenzenesulfonamide using phenyl ethyl chloride as a starting material and producing as an intermediate N-mesyl-4-(2-chloroethyl)benzenesulfonamide. Analysis of obtained vs. theoretical values for the intermediate are as follows: melting point: 149°-151° C.; neutralization equivalent: 302.05 (theory 297).

Sources & evidence

ORD record
ord-7a9abc3c4f704b6a8dd5f35f3c7155cd
Source dataset
uspto-grants-1985_04
Patent number
US04510324

Reaction notes

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