Ammonia → HCID 178483215, compound

HRID 1980707Notes

Reaction equation

HRID 1980707 reaction equation
CO[C:3]1[C:7](OC)=[N:6][S:5](=[O:11])(=[O:10])[N:4]=1.[CH3:12][N:13]([CH2:15][C:16]1[CH:17]=[C:18]([CH:24]=[CH:25][CH:26]=1)[O:19][CH2:20][CH2:21][CH2:22][NH2:23])[CH3:14].[NH3:27]>>[CH3:12][N:13]([CH2:15][C:16]1[CH:17]=[C:18]([CH:24]=[CH:25][CH:26]=1)[O:19][CH2:20][CH2:21][CH2:22][NH:23][C:7]1[C:3]([NH2:27])=[N:4][S:5](=[O:10])(=[O:11])[N:6]=1)[CH3:14]

Participants

4

Reactant 3

HCID 222AmmoniaHCID 122305383,4-Dimethoxy-1,2,5-thiadiazole 1,1-dioxideHCID 129139503-(3-Aminopropoxy)-N,N-dimethylbenzenemethanamine

Product 1

HCID 178483215HCID 178483215, compound

Procedure

When a methanolic suspension of 3,4-dimethoxy-1,2,5-thiadiazole 1,1-dioxide is successively treated with an equimolar amount of 3-[3-(dimethylaminomethyl)phenoxy]propylamine [prepared according to the procedure described in Belgian Pat. No. 867,106] and excess ammonia by the general procedure described in Example 35, the title compound is thereby produced.

Workup

  1. customprepared

Sources & evidence

ORD record
ord-24f45af6920943e09a358c064a7948ba
Source dataset
uspto-grants-1985_04
Patent number
US04510309

Reaction notes

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